1-甲氧基-1,3-环己二烯合成路线 （共 48 条）
反应条件
hydrogenchloride; tetrabutyl ammonium fluoride; water in dichloromethane T=0°C;
参考文献
Tetrahedron Letters, , vol. 36, # 42 p. 7765 - 7766
反应条件
1: 30 percent / 96 h / 130 °C 2: 86 percent / lithium aluminum hydride / diethyl ether / 2 h / Heating 3: 97 percent / phosphorus tribromide / CH2Cl2 / 4 h / Heating 4: 79 percent / lithium aluminum hydride / toluene / 0.5 h / Heating 5: 43 percent / conc. HNO3; conc. H2SO4 / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Knoelker, Hans-Joachim; Baum, Elke; Hopfmann, Thomas
Tetrahedron, 1999 , vol. 55, # 34 p. 10391 - 10412
反应条件
T=160°C; Diels-Alder reaction; 8 h;
参考文献
Ashburn, Bradley O.; Carter, Rich G.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 2 p. 255 - 257
反应条件
sodium in ammonia; water; methoxybenzene
参考文献
Givaudan Corporation
Patent: US3962354 A1, 1976 ;
反应条件
Behandeln der Reaktionsloesung mit wss. Ammoniumchlorid-Loesung;
参考文献
Birch
Journal of the Chemical Society, 1950 , p. 1551,1554
参考文献
Schnur; Morville
Journal of Medicinal Chemistry, 1986 , vol. 29, # 5 p. 770 - 778
反应条件
1: 83 percent / methanol / 1 h / Ambient temperature 2: 1.) NaH, 2.) Ag2O, MgSO4 / 1.) THF, 0 deg C, 30 min, 2.) THF, 1.5 h 3: 83 percent / p-toluenesulfonic acid / xylene / 1.25 h / Heating 4: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h / Ambient temperature View Scheme
参考文献
Tapia, Ricardo; Valderrama, Jaime A.; Quintanar, Carmina
Heterocycles, 1994 , vol. 38, # 8 p. 1797 - 1804
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Krohn, Karsten
Tetrahedron Letters, 1980 , vol. 21, p. 3557 - 3560
参考文献
Birch; Hextall
Australian Journal of Chemistry, 1955 , vol. 8, p. 96,99
反应条件
[Ru(C=C=CPh2)Cp(1,3,5-triaza-7-phosphaadamantane)(PPh3)](CF3SO3) in chloroform-d1; water-d2 T=20°C; 2 h; Inert atmosphere;
参考文献
Serrano-Ruiz, Manuel; Lidrissi, Chaker; Manas, Sonia; Peruzzini, Maurizio; Romerosa, Antonio
Journal of Organometallic Chemistry, 2014 , vol. 751, p. 654 - 661
