2,4-二甲氧基苯甲酸甲酯合成路线 （共 31 条）
参考文献
Van Otterlo, Willem A. L.; Michael, Joseph P.; De Koning, Charles B.
Synthetic Communications, 2007 , vol. 37, # 20 p. 3611 - 3621
反应条件
potassium carbonate in acetone 24 h; Heating;
参考文献
Anderson, Wayne K.; Boehm, Terri L.; Makara, Gergely M.; Swann, R. Thomas
Journal of Medicinal Chemistry, 1996 , vol. 39, # 1 p. 46 - 55
反应条件
copper quinolate; tetra-(n-butyl)ammonium iodide in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
sulfuric acid 14 h; Heating / reflux;
参考文献
WO2006/87077 A2, ;
Page/Page column 84 ;
反应条件
potassium phosphate; copper quinolate; tetra-(n-butyl)ammonium iodide in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
1: 4-methoxy-2-methoxy benzoic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 0.5 h; 2: methanol With sodium tetrahydroborate in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Synthesis, , # 9 art. no. M12811SS, p. 1375 - 1382
反应条件
1: 9 percent / manganese(III) acetate / acetic acid / 0.02 h / Heating 2: methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 2 p. 545 - 550
反应条件
2: 9 percent / manganese(III) acetate / acetic acid / 0.02 h / Heating 3: methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 2 p. 545 - 550
反应条件
in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 23 p. 3041 - 3044
反应条件
in dimethyl sulfoxide T=20°C; 5 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 51, # 23 p. 3041 - 3044
