2,6-二甲基苯基溴化镁合成路线 （共 31 条）
反应条件
1: 97 percent Chromat. / Cs2CO3; Pd(OAc)2; PCy3 / o-xylene / 4 h / Heating
View Scheme
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
反应条件
boron trifluoride diethyl etherate in diethyl ether
T=100°C; 3 h;
参考文献
Lapkin, I. I.; Yuzhakova, G. A.; Drovneva, R. P.; Andriyanova, N. V.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 2 p. 368 - 371,301 - 303
反应条件
C46H55ClFeN3Pd; lithium chloride in tetrahydrofuran
T=60°C; Kumada coupling reaction; 24 h; Inert atmosphere;
参考文献
Ren, Gerui; Cui, Xiuling; Wu, Yangjie
European Journal of Organic Chemistry, 2010 , # 12 p. 2372 - 2378
反应条件
in tetrahydrofuran
3 h; Heating;
参考文献
Vinod; Hart
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 881 - 890
参考文献
Watanabe, Soichiro; Goto, Kei; Kawashima, Takayuki; Okazaki, Renji
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7677 - 7680
参考文献
De Winter; Nauta
European Journal of Medicinal Chemistry, 1977 , vol. 12, # 2 p. 125 - 130
反应条件
C54H80Cl2Fe2N2O4 in diethyl ether
T=100°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Qian, Xin; Dawe, Louise N.; Kozak, Christopher M.
Dalton Transactions, 2011 , vol. 40, # 4 p. 933 - 943
反应条件
C54H80Cl2Fe2N2O4 in diethyl ether
T=100°C; 0.166667 h; Inert atmosphereMicrowave irradiation;
参考文献
Qian, Xin; Dawe, Louise N.; Kozak, Christopher M.
Dalton Transactions, 2011 , vol. 40, # 4 p. 933 - 943
反应条件
C54H80Cl2Fe2N2O4 in diethyl ether
T=22°C; 0.5 h; Inert atmosphere;
参考文献
Qian, Xin; Dawe, Louise N.; Kozak, Christopher M.
Dalton Transactions, 2011 , vol. 40, # 4 p. 933 - 943
反应条件
C46H55ClFeN3Pd; lithium chloride in tetrahydrofuran
T=60°C; Kumada coupling reaction; 24 h; Inert atmosphere;
参考文献
Ren, Gerui; Cui, Xiuling; Wu, Yangjie
European Journal of Organic Chemistry, 2010 , # 12 p. 2372 - 2378
