3-甲基-2-环己烯-1-醇合成路线 (共 78 条)
反应条件
sodium tetrahydroborate; alpha-cyclodextrin in water influence of other cyclodextrin on the reduction; Product distribution;
参考文献
Chemistry Letters, , p. 1117 - 1118
反应条件
in tetrahydrofuran 18 h; -70 deg C to r.t.;
参考文献
Tetrahedron Letters, , vol. 31, # 4 p. 511 - 514
反应条件
oxygen T=60°C; P=760 Torr; 27 h; var. cond. of autooxidation, solvent, oxidizing agents, other methylsubstituted cyclohexene; Product distributionMechanism;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 17 p. 1227 - 1229
反应条件
oxygen; molybdenum hexacarbonyl T=95°C; 3 h; further reaction time, temperature; Product distribution;
参考文献
Journal of applied chemistry of the USSR, , vol. 58, # 10 pt 2 p. 2133 - 2140
参考文献
Journal of the Chemical Society, , p. 131,136, 141
反应条件
bromine; 2,3-dimethyl aniline 1) dichloromethane, -60 deg C, 2) dichloromethane, -40 deg C; Yield given. Multistep reaction;
参考文献
Bhandal, Harcharan; Patel, Vinod F.; Pattenden, Gerald; Russell, Jamie J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 10 p. 2691 - 2701
反应条件
cerium(III) chloride 0.3 h; Heating;
参考文献
Uzarewicz; Dresler
Polish Journal of Chemistry, 1998 , vol. 72, # 8 p. 1921 - 1930
反应条件
pyridine; oxygen in hexane 0.166667 h; UV-irradiation; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Clennan, Edward L.; Zhang, Dong; Singleton, Jamie
Photochemistry and Photobiology, 2006 , vol. 82, # 5 p. 1226 - 1232
反应条件
1: pyridine / 96 h / Ambient temperature 2: H2 / ruthenium View Scheme
参考文献
Hirano, Masao; Morimoto, Takashi
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1105 - 1108
反应条件
3-[{2-[4-(4-{2-[bis-(2-methoxycarbonyl-ethyl)-amino]-ethylcarbamoyl}-phenyldisulfanyl)-benzoylamino]-ethyl}-(2-methoxycarbonyl-ethyl)-amino]-propionic acid methyl ester in benzene T=20°C; 12 h; UV-irradiation;
参考文献
Tsuboi, Takaaki; Takaguchi, Yutaka; Tsuboi, Sadao
Heteroatom Chemistry, 2009 , vol. 20, # 1 p. 1 - 11