2-(2-苯基乙基)吡啶合成路线 （共 33 条）
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; sodium carbonate; mTPPDS; sodium lauryl sulfate
T=80°C; 6 h;
参考文献
Lautens; Roy; Fukuoka; Fagnou; Martin-Matute
Journal of the American Chemical Society, 2001 , vol. 123, # 22 p. 5358 - 5359
反应条件
1: With sodium in tetrahydrofuran
T=0°C; 12 h;
2: With water in tetrahydrofuran
cooling;
参考文献
Azzena, Ugo; Dettori, Giovanna; Lubinu, Caterina; Mannu, Alberto; Pisano, Luisa
Tetrahedron, 2005 , vol. 61, # 36 p. 8663 - 8668
反应条件
hydrogen; triethylamine; palladium on activated charcoal in ethanol
参考文献
Tilley, Jefferson W.; Zawoiski, Sonja
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 386 - 390
反应条件
1: 2-picoline With lithium diisopropyl amide in tetrahydrofuran; hexane
T=20°C; 1 h;
2: benzyl bromide in tetrahydrofuran; hexane
T=0°C; 0.5 h;
参考文献
Alunni, Sergio; De Angelis, Filippo; Ottavi, Laura; Papavasileiou, Magdalini; Tarantelli, Francesco
Journal of the American Chemical Society, 2005 , vol. 127, # 43 p. 15151 - 15160
反应条件
triphenyl phosphite; methanol; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in toluene
T=120°C; 24 h;
参考文献
Ogiwara, Yohei; Kochi, Takuya; Kakiuchi, Fumitoshi
Organic Letters, 2011 , vol. 13, # 12 p. 3254 - 3257
反应条件
[(1,5-cyclooctadiene)Ir(μ2-OH)]2; potassium tert-butylate; triphenylphosphine in 1,4-dioxane
T=130°C; 24 h; Inert atmosphere;
参考文献
Obora, Yasushi; Ogawa, Shinji; Yamamoto, Nobuyuki
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 9429 - 9433,5
反应条件
bromobenzene; diethyl ether; lithium
anschl. mit Benzylchlorid;
参考文献
Osuch; Levine
Journal of the American Chemical Society, 1956 , vol. 78, p. 1723
反应条件
C41H38BFeN3P2; hydrogen in tetrahydrofuran
T=20 - 90°C; P=3000.3 Torr; 48 h; Inert atmosphere;
参考文献
Srimani, Dipankar; Diskin-Posner, Yael; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2013 , vol. 52, # 52 p. 14131 - 14134
Angew. Chem., 2013 , vol. 125, # 52 p. 14381 - 14383
反应条件
(NH4)2S2O8; silver nitrate; trifluoroacetic acid in water
T=70°C; Minisci reaction; 6 h;
参考文献
Burgin, Ryan N.; Jones, Simon; Tarbit
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6772 - 6774
反应条件
1: (2-iodoethyl)-benzene With indium; copper(l) chloride in tetrahydrofuran
T=20°C; 24 h;
2: 2-bromo-pyridine With bis-triphenylphosphine-palladium(II) chloride; lithium chloride in N,N-dimethyl acetamide
T=100°C; 24 h;
参考文献
Shen, Zhi-Liang; Goh, Kelvin Kau Kiat; Yang, Yong-Sheng; Lai, Yin-Chang; Wong, Colin Hong An; Cheong, Hao-Lun; Loh, Teck-Peng
Angewandte Chemie - International Edition, 2011 , vol. 50, # 2 p. 511 - 514
