三乙氧基(4-甲氧苯基)硅烷合成路线 （共 36 条）
反应条件
triethylamine; [Rh(NCMe)2(cod)][BF4] in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Murata, Miki; Yamasaki, Hiyoruki; Ueta, Tsukasa; Nagata, Masayuki; Ishikura, Masanori; Watanabe, Shinji; Masuda, Yuzuru
Tetrahedron, 2007 , vol. 63, # 19 p. 4087 - 4094
反应条件
[Rh(NCMe)2(cod)][BF4]; triethylamine in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Murata, Miki; Ishikura, Masanori; Nagata, Masayuki; Watanabe, Shinji; Masuda, Yuzuru
Organic Letters, 2002 , vol. 4, # 11 p. 1843 - 1845
反应条件
1: 4-methoxybenzenediazonium tosylate With [RhCl(η2:η2-cycloocta-1,5-diene)]2; tetra-(n-butyl)ammonium iodide; triethylamine in N,N-dimethyl-formamide T=20°C; Sandmeyer reaction; 2 h; Inert atmosphere; 2: 4-bromooctafluorobutanetriethoxysilane in N,N-dimethyl-formamide T=20 - 100°C; Inert atmosphere;
参考文献
Tang, Zhi Yong; Zhang, Yuan; Wang, Tao; Wang, Wei
Synlett, 2010 , # 5 art. no. W16209ST, p. 804 - 808
反应条件
N-ethyl-N,N-diisopropylamine; biphenyl-2-yl-di-tert-butyl-phosphane; bis(dibenzylideneacetone)-palladium(0) in 1-methyl-pyrrolidin-2-one T=20°C; 12 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Journal of Organic Chemistry, , vol. 66, # 22 p. 7449 - 7455
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=20°C; sonochemical Barbier-type reaction; 0.5 h; Irradiationsonication; Product distribution; Further Variations:reagent ratio;
参考文献
Lee, Adam Shih-Yuan; Chang, Yu-Ting; Chu, Shu-Fang; Tsao, Kuo-Wei
Tetrahedron Letters, 2006 , vol. 47, # 39 p. 7085 - 7087
反应条件
tetra-(n-butyl)ammonium iodide; triethylamine; [Rhacetylacetonate(1,5-cyclooctadiene)] in N,N-dimethyl-formamide T=100°C; 16 h;
参考文献
Murata, Miki; Yamasaki, Hiyoruki; Ueta, Tsukasa; Nagata, Masayuki; Ishikura, Masanori; Watanabe, Shinji; Masuda, Yuzuru
Tetrahedron, 2007 , vol. 63, # 19 p. 4087 - 4094
反应条件
1: 1-bromo-4-methoxy-benzene With magnesium in tetrahydrofuran T=20°C; 2: ethyl orthosilicate in tetrahydrofuran T=0 - 20°C; 13 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 24 p. 8305 - 8314
反应条件
1.1: magnesium / tetrahydrofuran / 20 °C 1.2: SiCl4 / tetrahydrofuran 2.1: 70 percent Chromat. / pyridine / -30 - 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 24 p. 8305 - 8314
反应条件
pyridine T=-30 - 0°C;
参考文献
Journal of Organic Chemistry, , vol. 69, # 24 p. 8305 - 8314
参考文献
Journal of Organometallic Chemistry, , vol. 685, # 1-2 p. 93 - 98
