1-叔丁氧基-4-硝基苯合成路线 (共 23 条)
反应条件
(1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=20°C; 9 h;
参考文献
Kataoka, Noriyasu; Shelby, Quinetta; Stambuli, James P.; Hartwig, John F.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5553 - 5566
反应条件
potassium hexamethylsilazane in tetrahydrofuran T=0 - 23°C; 2 h;
参考文献
Woiwode, Thomas F.; Rose, Christoph; Wandless, Thomas J.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9594 - 9596
反应条件
(1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=20°C; 5 h;
参考文献
Kataoka, Noriyasu; Shelby, Quinetta; Stambuli, James P.; Hartwig, John F.
Journal of Organic Chemistry, 2002 , vol. 67, # 16 p. 5553 - 5566
反应条件
in hexane; ethyl acetate
参考文献
Yale University
Patent: US6562989 B2, 2003 ;
反应条件
in tetrahydrofuran T=0 - 23°C; 2 h;
参考文献
Woiwode, Thomas F.; Rose, Christoph; Wandless, Thomas J.
Journal of Organic Chemistry, 1998 , vol. 63, # 25 p. 9594 - 9596
反应条件
2,6-dimethyl-1,4-benzoquinone in dichloromethane 10 h; Heating;
参考文献
Shintou, Taichi; Kikuchi, Wataru; Mukaiyama, Teruaki
Chemistry Letters, 2003 , vol. 32, # 1 p. 22 - 23
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Shintou, Taichi; Mukaiyama, Teruaki
Journal of the American Chemical Society, 2004 , vol. 126, # 23 p. 7359 - 7367
反应条件
N,N-tetramethylene-thiocarbamoyl-sulphenamide in N,N-dimethyl-formamide T=20°C; 0.333333 h;
参考文献
Makosza, Mieczyslaw; Bialecki, Maciej
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 4878 - 4888
反应条件
1: tert-butyl alcohol With sodium t-butanolate in toluene T=0 - 20°C; 0.25 h; Inert atmosphere; 2: (4-nitrophenyl)(phenyl)iodonium triflate in toluene T=0 - 20°C; Inert atmosphere; chemoselective reaction;
参考文献
Ghosh, Raju; Lindstedt, Erik; Jalalian, Nazli; Olofsson, Berit
ChemistryOpen, 2014 , vol. 3, # 2 p. 54 - 57
反应条件
boron trifluoride diethyl etherate in dichloromethane; cyclohexane 16 h; Ambient temperature;
参考文献
Armstrong, Alan; Brackenridge, Ian; Jackson, Richard F.W.; Kirk, Joanna M.
Tetrahedron Letters, 1988 , vol. 29, # 20 p. 2483 - 2486
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=-35°C; 0.333333 h;
参考文献
Makosza, Mieczyslaw; Sypniewski, Michal
Tetrahedron, 1994 , vol. 50, # 16 p. 4913 - 4920