1.1: hydrogenchloride; calcium chloride; sodium hypochlorite / dichloromethane; water / 0.25 h / -30 - -25 °C 1.2: 0.5 h / 0 °C / |Cooling with acetone-dry ice 2.1: N-chloro-succinimide; oxygen; copper dichloride / acetonitrile / 16 h / 130 °C / 760.05 Torr 3.1: magnesium / methanol / 20 °C / |Sonication View Scheme
参考文献
Urones, Beatriz; Martinez, Angel Manu; Rodriguez, Nuria; Arrayas, Ramon Gomez; Carretero, Juan C.
Chemical Communications, 2013 , vol. 49, # 94 p. 11044 - 11046