N,N,O-三(三甲基硅基)羟胺合成路线 （共 4 条）
反应条件
(i) nBuLi, THF, hexane, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Nowakowski,P.; West,R.
Journal of the American Chemical Society, 1976 , vol. 98, p. 5616 - 5620
反应条件
ethanol in ethanol byproducts: EtOSiMe3; stirring of neat (Me3Si)2NOSiMe3 and Ge-compound (20°C, 12 h), distn. (1-2 Torr), addn. of EtOH to residue (20-30°C), evapn. after 12 h; recrystn. (ethyl acetate); elem. anal.;
参考文献
Kozyukov, Vik. P.; Feoktistov, A. E.; Mironov, V. F.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 937 - 939
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 1056 - 1059
反应条件
ethanol 1.) 20 deg C, 12 h; 2.) 20 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Kozyukov, Vik. P.; Feoktistov, A. E.; Mironov, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 6 p. 1299 - 1304,1154 - 1158
反应条件
phosphorus oxotrifluoride
参考文献
Lidy,W. et al.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1977 , vol. 32, p. 595 - 596
