2,6-二叔丁基-4-溴甲基苯酚合成路线 （共 25 条）
反应条件
in tetrahydrofuran T=85°C; 4 - 5 h;
参考文献
Council of Scientific and Industrial Research
Patent: US6770785 B1, 2004 ;
Location in patent: Page column 6 ;
反应条件
triethylamine in pentane T=6°C; few minutes;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 306 - 312
反应条件
1: Et3N / pentane / 6 °C / few minutes 2: 4 percent / pentane / 30 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 1 p. 306 - 312
参考文献
Cook et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 1783
反应条件
in methanol 1 h; Heating;
参考文献
Gorbunov, D. B.; Voznesenskii, V. N.; Ershov, V. V.; Nikiforov, G. A.
Russian Chemical Bulletin, 1994 , vol. 43, # 1 p. 93 - 97
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 1 p. 98 - 102
反应条件
1: Et3N / pentane / 6 °C / few minutes 2: 6 percent / pentane / 30 °C View Scheme
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 306 - 312
反应条件
1: methanol 2: bromine; acetic acid View Scheme
参考文献
Fujisaki
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 727,729
Chem.Abstr., 1958 , p. 8096
反应条件
4-(N,N-dimethlyamino)pyridine in N,N-dimethyl-formamide
参考文献
Kang, Tae-Souk; Jo, Hyang-Ok; Park, Woo-Kyu; Kim, Jong-Pyung; Konishi, Yasuo; Kong, Jae-Yang; Park, No-Sang; Jung, Young-Sik
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 5 p. 1663 - 1667
参考文献
Rieker,A.; Kessler,H.
Tetrahedron, 1968 , vol. 24, p. 5133 - 5144
反应条件
1: H2O; acetone 2: aq. NaOH View Scheme
参考文献
Rieker,A. et al.
Tetrahedron, 1968 , vol. 24, p. 103 - 115
