1.1: N-chlorosuccinimide; pyridine / tetrahydrofuran / 0.5 h / 60 °C
1.2: triethylamine / tetrahydrofuran / 2 h / 50 °C
2.1: pyridinium chlorochromate; silica gel / CH2Cl2 / 5 h
View Scheme
参考文献
Landge, Kamalkishor P.; Oh, Ji Seon; Pae, Ae Nim; Park, Woo Kyu; Gong, Jae Yang; Koh, Hun Yeong; Jung, Sun Ho
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 7 p. 2449 - 2452
1: piperonal oxime With pyridine; N-chloro-succinimide in tetrahydrofuran
T=60°C; 0.5 h;
2: propargyl alcohol With triethylamine in tetrahydrofuran
T=50°C; 2 h;
参考文献
Landge, Kamalkishor P.; Oh, Ji Seon; Pae, Ae Nim; Park, Woo Kyu; Gong, Jae Yang; Koh, Hun Yeong; Jung, Sun Ho
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 7 p. 2449 - 2452
