(2-甲氧基-6-硝基苯基)乙腈合成路线 (共 17 条)
反应条件
1: SOCl2 2: aqueous ethanol View Scheme
参考文献
Yakugaku Zasshi, , vol. 79, p. 723,726
Chem.Abstr., , p. 22041
反应条件
sulfuric acid 16 h; Reflux;
参考文献
F2G LIMITED
Patent: US2011/9390 A1, 2011 ;
Location in patent: Page/Page column 23 ;
反应条件
hydrogen; acetic acid; 10 palladium on active carbon in ethanol P=2280 Torr; 2 h; Ambient temperature;
参考文献
Makosza, Mieczyslaw; Danikiewicz, Witold; Wojciechowski, Krzysztof
Liebigs Annalen der Chemie, 1988 , p. 203 - 208
反应条件
1: 97 percent / aq. HCl; H2SO4 2: 97 percent / H2 / 10 percent Pd/C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 20 p. 2957 - 2961
反应条件
1: aqueous HCl 2: palladium; acetic acid / Hydrogenation 3: methanol. sodium methylate / Behandeln des Reaktionsprodukts mit wss.Natronlauge 4: lithium alanate; diethyl ether View Scheme
参考文献
Cook et al.
Journal of the Chemical Society, 1952 , p. 3904,3909
反应条件
1: 97 percent / aq. HCl; H2SO4 2: 97 percent / H2 / 10 percent Pd/C 3: 73 percent / 48 percent aq. HBr View Scheme
参考文献
Steffan, Robert J.; Ashwell, Mark A.; Solvibile, William R.; Matelan, Edward; Largis, Elwood; Han, Stella; Tillet, Jeffery; Mulvey, Ruth
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 20 p. 2957 - 2961
反应条件
hydrogenchloride; sulfuric acid
参考文献
Steffan, Robert J.; Ashwell, Mark A.; Solvibile, William R.; Matelan, Edward; Largis, Elwood; Han, Stella; Tillet, Jeffery; Mulvey, Ruth
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 20 p. 2957 - 2961