(2-甲氧基-6-硝基苯基)乙腈合成路线 （共 17 条）
参考文献
Steffan, Robert J.; Ashwell, Mark A.; Solvibile, William R.; Matelan, Edward; Largis, Elwood; Han, Stella; Tillet, Jeffery; Mulvey, Ruth
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 20 p. 2957 - 2961
反应条件
in ethanol 16 h; Reflux;
参考文献
F2G LIMITED
Patent: US2011/9390 A1, 2011 ;
Location in patent: Page/Page column 23 ;
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=-20 - -10°C; 0.5 h;
参考文献
Makosza, Mieczyslaw; Danikiewicz, Witold; Wojciechowski, Krzysztof
Liebigs Annalen der Chemie, 1988 , p. 203 - 208
反应条件
potassium tert-butylate in N,N-dimethyl-formamide T=-20°C; 2 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 7 p. 1149 - 1166
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.17 h / 20 °C 1.2: 5 h / 65 °C 2.1: potassium tert-butylate / N,N-dimethyl-formamide / 2 h / -20 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 7 p. 1149 - 1166
反应条件
1: NaOMe / methanol 2: NBS, (PhCO)2O2 / CCl4 / Irradiation 3: aq. ethanol View Scheme
参考文献
Tetrahedron, , vol. 24, p. 6093 - 6109
反应条件
1: NBS, (PhCO)2O2 / CCl4 / Irradiation 2: aq. ethanol View Scheme
参考文献
Tetrahedron, , vol. 24, p. 6093 - 6109
反应条件
1: (i) NaNO2, aq. H2SO4, (ii) CuSO4 2: NaOMe / methanol 3: NBS, (PhCO)2O2 / CCl4 / Irradiation 4: aq. ethanol View Scheme
参考文献
Tetrahedron, , vol. 24, p. 6093 - 6109
参考文献
Journal of the Chemical Society, , p. 3904,3909
Yakugaku Zasshi, , vol. 79, p. 723,726
Chem.Abstr., , p. 22041
反应条件
1: SOCl2 / anschliessende Umsetzung mit NaBH4 in THF 2: SOCl2 3: aqueous ethanol View Scheme
参考文献
Yakugaku Zasshi, , vol. 79, p. 723,726
Chem.Abstr., , p. 22041
