三[2-(三甲基硅氧基)乙基]胺合成路线 (共 23 条)
反应条件
sulfuric acid in dichloromethane T=20°C; 11 h;
参考文献
Lakouraj; Akbari
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 5 p. 1165 - 1167
反应条件
triethylamine in chloroform
参考文献
Lukevits,E. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, p. 1462 - 1467,1432 - 1436
参考文献
Fridland,D.V. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 2 p. 326 - 329,324 - 327
反应条件
T=140 - 150°C; Yields of byproduct given;
参考文献
Voronkov, M. G.; Kuznetsova, G. A.; Baryshok, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 7 p. 1682,1512 - 1513
反应条件
hydrogen fluoride T=7 - 8°C; Fluorination; cyclization; 8.41667 h; Electrochemical reaction;
参考文献
Abe, Takashi; Soloshonok, Irina; Baba, Hajime; Sekiya, Akira
Journal of Fluorine Chemistry, 1999 , vol. 99, # 1 p. 51 - 57
反应条件
in n-heptane byproducts: Me3SiCl; amine was added to soln. of EtGeCl3 in heptane at 60-70°C; mixt. was stirred at room temp.; evapd. (vac.); recrystd. (toluene);
参考文献
Chernyshev; Knyazev; Kirin; Vasilev; Alekseev
Russian Journal of General Chemistry, 2004 , vol. 74, # 1 p. 58 - 65
反应条件
T=140 - 150°C; Yields of byproduct given;
参考文献
Voronkov, M. G.; Kuznetsova, G. A.; Baryshok, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 7 p. 1682,1512 - 1513
反应条件
T=140 - 150°C; Yields of byproduct given;
参考文献
Voronkov, M. G.; Kuznetsova, G. A.; Baryshok, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 7 p. 1682,1512 - 1513
反应条件
in hexane
T=20°C; 0.166667 h;
参考文献
Voronkov; Albanov; Grebneva; Trofimova; Chernov; Chipanina
Russian Journal of General Chemistry, 2006 , vol. 76, # 12 p. 1854 - 1859
反应条件
T=140 - 150°C; Yields of byproduct given;
参考文献
Voronkov, M. G.; Kuznetsova, G. A.; Baryshok, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 7 p. 1682,1512 - 1513