4-羟基-3-丁烯酸 gamma-内酯合成路线 (共 8 条)
反应条件
5 wt Ru/carbon; hydrogen in water T=125 - 175°C;
参考文献
Vispute, Tushar P.; Huber, George W.
Green Chemistry, 2009 , vol. 11, # 9 p. 1433 - 1445
反应条件
T=300 - 800°C; Mechanism;
参考文献
Xu, Zhi Ping; Mok, Chup Yew; Chin, Wee Shong; Huang, Hsing Hua; Li, Sheng; Huang, Wei
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 4 p. 725 - 729
参考文献
Merck and Co., Inc.
Patent: US6476041 B1, 2002 ;
US 6476041 B1
反应条件
triethylamine in acetonitrile T=60°C; 10 h;
参考文献
Nasman
Synthesis, 1985 , vol. NO. 8, p. 788 - 789
反应条件
T=300 - 800°C; Mechanism;
参考文献
Xu, Zhi Ping; Mok, Chup Yew; Chin, Wee Shong; Huang, Hsing Hua; Li, Sheng; Huang, Wei
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 4 p. 725 - 729
反应条件
sodium monohydrogen sulfate; sodium ethanolate; toluene-4-sulfonic acid in ethanol; cyclohexane; ethylene glycol
参考文献
Henkel Corporation
Patent: US5103026 A1, 1992 ;
反应条件
1: 2-chlorophenol With sodium ethanolate in ethanol
0.0833333 h;
2: (5H)-furan-2-one in ethanol
T=100 - 150°C; 17 h;
3: With hydrogenchloride; ethanol; water
参考文献
Dehmlow, Henrietta; Grether, Uwe; Kratochwil, Nicole A.; Narquizian, Robert; Panousis, Constantinos
Patent: US2007/72873 A1, 2007 ;
Location in patent: Page/Page column 16 ;
US 20070072873 A1
反应条件
hydroquinone; mercury
参考文献
Synthelabo
Patent: US4172143 A1, 1979 ;