4-[(三甲基甲硅烷基)氧基]-苯甲酸三甲基硅酯合成路线 （共 9 条）
反应条件
triethylamine in toluene 2 h; Heating;
参考文献
Schwarz, Gerd; Alberts, Heinrich; Kricheldorf, Hans R.
Liebigs Annalen der Chemie, 1981 , # 7 p. 1257 - 1270
参考文献
Skorokhodov, S. S.; Korshun, A. M.; Asinovskaja, D. N.
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 155, p. 179 - 188
反应条件
pyridine T=20°C; 1 h;
参考文献
Krafczyk, Nicole; Glomb, Marcus A.
Journal of Agricultural and Food Chemistry, 2008 , vol. 56, # 9 p. 3368 - 3376
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
参考文献
Dannley,R.L.; Knipple,W.R.
Journal of Organic Chemistry, 1973 , vol. 38, # 1 p. 6 - 11
反应条件
1: 4-methoxy-benzoic acid With cytochrome P450 enzyme CYP199A4 from Rhodopseudomonas palustris HaA2; nicotinamide adenine dinucleotide; bovine liver catalase in ethanol pH=7.4; Enzymatic reaction; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With chloro-trimethyl-silane in acetonitrile 2 h;
参考文献
Bell, Stephen G.; Zhou, Ruimin; Yang, Wen; Tan, Adrian B. H.; Gentleman, Alexander S.; Wong, Luet-Lok; Zhou, Weihong
Chemistry - A European Journal, 2012 , vol. 18, # 52 p. 16677 - 16688
反应条件
1: 60 percent / SOCl2 / CH2Cl2 / 3 h / Heating 2: 1) triethylamine / 1) methylene chloride, 30 min, reflux, 2) methylene chloride, 30 min, reflux 3: 63 percent / CHCl3 / 2 h / Ambient temperature View Scheme
参考文献
Schwarz, Gerd; Alberts, Heinrich; Kricheldorf, Hans R.
Liebigs Annalen der Chemie, 1981 , # 7 p. 1257 - 1270
反应条件
triethylamine in neat (no solvent) in presence of a few HF, CsF, KF, (R4N)F, (C2H5)2NH, effectless in presence of pyridinp, NaF and NH4F;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.4, page 137 - 166
反应条件
1: 60 percent / SOCl2 / CH2Cl2 / 3 h / Heating 2: 2) ethyl acetate / 1) methylene chloride, 30 min, reflux, 2) THF View Scheme
参考文献
Schwarz, Gerd; Alberts, Heinrich; Kricheldorf, Hans R.
Liebigs Annalen der Chemie, 1981 , # 7 p. 1257 - 1270
