[Me4N][BF4] in acetonitrile
T=30°C; electrochemical reaction; Further byproducts given. Title compound not separated from byproducts;
参考文献
Ahmad, Iftikhar; Bethell, Donald; Parker, Vernon D.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 9 p. 1527 - 1530
Saitoh, Yasuo; Kaneko, Makoto; Segawa, Katsunori; Itoh, Hiroki; Sakuragi, Hirochika
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 9 p. 2013 - 2023
1: 78 percent / hydrazine hydrate / pyridine / 12 h / 50 °C
2: 14 percent / NaOH / ethanol; H2O / 20 h / Heating
View Scheme
参考文献
Minabe, Masahiro; Nozawa, Toshiya; Kurose, Tomoko; Kimura, Takao; Tsubota, Motohiro
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 3 p. 693 - 697
zinc(II) chloride in diethyl ether
1 h; Ambient temperature;
参考文献
Anjaneyulu, P. S. R.; Lala, Anil K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 802 - 807
Saitoh, Yasuo; Kaneko, Makoto; Segawa, Katsunori; Itoh, Hiroki; Sakuragi, Hirochika
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 9 p. 2013 - 2023