(R)-(-)-扁桃酸甲酯合成路线 （共 107 条）
反应条件
potassium hydroxide; isopropyl alcohol; lt;Rh(C6H10)Clgt;2*MeNHCH(Ph)CH(Ph)NHMe; silica gel Ambient temperature;
参考文献
Gamez, Patrick; Fache, Fabienne; Lemaire, Marc
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 600 - 602
反应条件
toluene-4-sulfonic acid 3 h; Heating;
参考文献
Favre, Annaick; Carreaux, Francois; Deligny, Michael; Carboni, Bertrand
European Journal of Organic Chemistry, 2008 , # 29 p. 4900 - 4907
反应条件
formic acid*triethylamine; Ru/(S,S)-DPEN/MCF in isopropyl alcohol T=20°C; 12 h;
参考文献
Huang, Xiaohua; Ying, Jackie Y.
Chemical Communications, 2007 , # 18 p. 1825 - 1827
反应条件
water; copper(II) sulfate in chloroform T=40°C; 0.5 h; Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 5 p. 932 - 934
反应条件
oxygen in chloroform T=20°C; 28 h; Resolution of racemate; enantioselective reaction;
参考文献
Salunke, Santosh B.; Babu, N.Seshu; Chen, Chien-Tien
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1234 - 1240
参考文献
White, Ronald E.; Miller, John P.; Favreau, Leonard V.; Bhattacharyya, Apares
Journal of the American Chemical Society, 1986 , vol. 108, # 19 p. 6024 - 6031
反应条件
1: With methanesulfonamide; β-AD-Mix; 1,4-bis(9-O-dihydroquinidine)phthalazine in water; tert-butyl alcohol T=0°C; Oxidation; Sharpless asymmetric dihydroxylation; 2: With water; sodium sulfite in tert-butyl alcohol T=0 - 20°C; Reduction; 0.75 h;
参考文献
Monenschein, Holger; Draeger, Gerald; Jung, Alexander; Kirschning, Andreas
Chemistry - A European Journal, 1999 , vol. 5, # 8 p. 2270 - 2280
反应条件
hydrogenchloride in methanol T=4°C; 16 h;
参考文献
Elliott, John D.; Choi, Vanessa M. F.; Johnson, William S.
Journal of Organic Chemistry, 1983 , vol. 48, # 13 p. 2294 - 2295
反应条件
MCCD-HPS packed column in hydrogenchloride; acetonitrile pH=8.6;
参考文献
Analytical Chemistry, , vol. 75, # 6 p. 1348 - 1354
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; Esterification; 1 h;
参考文献
Parrish, Jay P.; Dueno, Eric E.; Kim, Seok-In; Jung, Kyung Woon
Synthetic Communications, 2000 , vol. 30, # 15 p. 2687 - 2700
