4-[(二苯基磷酰)甲基]吗啉合成路线 （共 6 条）
反应条件
1: methyl(diphenyl)phosphine oxide With Zn(2,2,6,6-tetramethylpiperidide)2 in toluene T=20°C; 1 h; 2: morpholino benzoate With [2,2']bipyridinyl; copper dichloride in tetrahydrofuran; toluene T=20°C;
参考文献
McDonald, Stacey L.; Wang, Qiu
Angewandte Chemie - International Edition, 2014 , vol. 53, # 7 p. 1867 - 1871
Angew. Chem., 2014 , vol. 126, # 7 p. 1898 - 1902,5
反应条件
hydrogenchloride T=80°C; Kabachnik-Fields reaction; 0.5 h; microwave irradiation;
参考文献
Prauda, Ibolya; Greiner, Istvan; Ludanyi, Krisztina; Keglevich, Gyoergy
Synthetic Communications, 2007 , vol. 37, # 2 p. 317 - 322
反应条件
in toluene 1 h; Heating;
参考文献
Broekhof, N. L. J. M.; Elburg, P. van; Gen, A. van der
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 11 p. 312 - 316
反应条件
in tetrahydrofuran 0.5 h;
参考文献
Broekhof, N. L. J. M.; Elburg, P. van; Gen, A. van der
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 11 p. 312 - 316
参考文献
Moehrle, Hans; Vetter, Wolfgang
Archiv der Pharmazie (Weinheim, Germany), 1989 , vol. 322, p. 427 - 430
反应条件
bis(trichloromethyl) carbonate Yield given. Multistep reaction;
参考文献
Pindur, Ulf; Otto, Christian
Tetrahedron, 1992 , vol. 48, # 17 p. 3515 - 3526
