Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2193 - 2194
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2336 - 2337
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反应条件
in sodium hydroxide aq. NaOH; High Pressure; hydrothermal; Ag sheets; less than stoichiometric amount of CoOOH; in O2 atmosphere at 330°C and 300 atm; 48-72 h;; treated with diluted nitric acid and washed with water, alcohol and ether; dried at 100°C;;
in neat (no solvent) byproducts: H2O, N2, C2H2; heated to 400°C with heating rate of 10°C and N2 flow of 30-100 mL/min or under O2 atm. (50 mL/min, 5 bars);
参考文献
Journal of Thermal Analysis and Calorimetry, , vol. 90, # 2 p. 517 - 523
Edwards, D. A.; Hayward, R. N.
Canadian Journal of Chemistry, 1968 , vol. 46, p. 3443 - 3446
Full Text Show Details
Gmelin Handbook: Ag: MVol.B5, 2.2.7.2, page 125 - 126
