1: (NH4)2S2O8; silver nitrate / acetonitrile; water / 80 °C
2: potassium hydroxide / methanol / 1 h / |Reflux
View Scheme
参考文献
Nasiri, Hamid Reza; Madej, M. Gregor; Panisch, Robin; Lafontaine, Michael; Bats, Jan W.; Lancaster, C. Roy D.; Schwalbe, Harald
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9530 - 9541
1: (NH4)2S2O8; silver nitrate / acetonitrile; water / 80 °C
2: potassium hydroxide / methanol / 1 h / |Reflux
View Scheme
参考文献
Nasiri, Hamid Reza; Madej, M. Gregor; Panisch, Robin; Lafontaine, Michael; Bats, Jan W.; Lancaster, C. Roy D.; Schwalbe, Harald
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9530 - 9541
1: 2-bromo-naphthalene-1,4-dione With sodium dithionite in tetrahydrofuran; water
T=20°C; 0.5 h; Inert atmosphere;
2: With potassium hydroxide in tetrahydrofuran; water
T=20°C; 1 h; Inert atmosphere;
3: dimethyl sulfate in tetrahydrofuran; water
T=20°C; 16 h; Inert atmosphere;
参考文献
Padwal, Jalindar; Lewis, William; Moody, Christopher J.
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 8082 - 8087
