2,6-二甲氧基苯甲酸甲酯合成路线 (共 22 条)
反应条件
sulfuric acid 18 h; Reflux;
参考文献
Moghaddam, Firouz Matloubi; Farimani, Mahdi Moridi
Tetrahedron Letters, 2010 , vol. 51, # 3 p. 540 - 542
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene 4 h; Heating;
参考文献
Shieh, Wen-Chung; Dell, Steven; Repic, Oljan
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2188 - 2191
反应条件
1: 1,3-dimethoxy benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
反应条件
hydrogenchloride in dimethyl carbonate (DMC); water
反应条件
copper quinolate in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
in various solvent(s) T=80°C; 2 h;
参考文献
Yoshino, Tomonori; Imori, Satomi; Togo, Hideo
Tetrahedron, 2006 , vol. 62, # 6 p. 1309 - 1317
反应条件
potassium carbonate in acetone 23 h; Heating;
参考文献
Tsuchida, Eishun; Hasegawa, Etsuo; Komatsu, Teruyuki; Nakata, Taisaku; Nishide, Hiroyuki
Chemistry Letters, 1990 , # 3 p. 389 - 392
反应条件
palladium diacetate; triphenylphosphine; p-benozquinone T=20°C; P=760.051 Torr; 5 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 2-3 p. 478 - 492
参考文献
Journal of the American Chemical Society, , vol. 62, p. 667