1-(2-甲氧基-5-甲基苯基)乙酮合成路线 （共 17 条）
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 0 - 20 °C
2: AlCl3, aluminium chloride / dichloromethane / 3 h / 0 - 20 °C
View Scheme
参考文献
JUBILANT BIOSYS LTD.; SARMA, Pakala Kumara Savithru; ACHARYA, Vinod Parameshwaran; KASIBHATLA, Srinivas Rao; VISWANADHAN, Vellarkad Narayana; TIWARI, Atul; SINGHA, Rakesh Kumar; BISCHOFF, Alexander
Patent: WO2012/90219 A2, 2012 ;
参考文献
v.Auwers
Justus Liebigs Annalen der Chemie, 1915 , vol. 408, p. 247
反应条件
Yield given. Multistep reaction;
参考文献
Kolis, Stanley P.; Kopach, Michael E.; Liu, Ronggang; Harman, W. Dean
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 130 - 136
参考文献
Noller; Adams
Journal of the American Chemical Society, 1924 , vol. 46, p. 1892
参考文献
v.Auwers; Lechner; Bundesmann
Chemische Berichte, 1925 , vol. 58, p. 41
反应条件
1: triethylamine / benzene
2: m-chloroperbenzoic acid / CH2Cl2 / -10 - 20 °C
3: 5.76 g / HCl / diethyl ether; H2O / 1 h
View Scheme
参考文献
Cong-Dung Le, Julie; Pagenkopf, Brian L.
Journal of Organic Chemistry, 2004 , vol. 69, # 12 p. 4177 - 4180
反应条件
diethyl ether; bromine; acetic acid
参考文献
Pendse; Limaye
Rasayanam, 1955 , vol. 2, p. 74,78
