3-(1,1-二甲基乙基)-环丁酮合成路线 （共 7 条）
反应条件
ammonium chloride; zinc in methanol 5 h;
参考文献
Broughton, Howard Barff; Dally, Robert Dean; Durham, Timothy Barrett; Gonzalez-Garcia, Maria Rosario; Sa, Lilly; Hahn, Patric James; Henry, Kenneth James; Kohn, Todd Jonathan; McCarthy, James Ray; Shepherd, Timothy Alan; Erickson, Jon Andre; Bueno Melendo, Ana Belen
Patent: US2007/225267 A1, 2007 ;
Location in patent: Page/Page column 51 ;
反应条件
1: allyl bromide With [Cp*2TiCl] in tetrahydrofuran T=-35°C; 0.0166667 h; 2: 2-methyl-2-iodopropane With samarium diiodide in tetrahydrofuran T=-35 - 20°C; 3: carbon monoxide in pentane T=45°C; P=517.162 Torr; 12 h; Further stages.;
参考文献
Carter; Greidanus; Chen; Stryker
Journal of the American Chemical Society, 2001 , vol. 123, # 36 p. 8872 - 8873
反应条件
1: zinc/copper couple; trichlorophosphate / diethyl ether / 40 °C 2: ammonium chloride; zinc / methanol / Reflux View Scheme
参考文献
Xu, Hua-Jian; Zhu, Feng-Fei; Shen, Yong-Ya; Wan, Xin; Feng, Yi-Si
Tetrahedron, 2012 , vol. 68, # 22 p. 4145 - 4151
参考文献
Salauen,J.; Conia,J.-M.
Bulletin de la Societe Chimique de France, 1968 , p. 3730 - 3735
反应条件
oxygen; pivalaldehyde
参考文献
Bolm, Carsten; Luong, T. Kim Khanh; Schlingloff, Gunther
Synlett, 1997 , vol. 1997, # 10 p. 1151 - 1152
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane
-78 deg C, 3 h then rt., 1 h;
参考文献
Baudin, J. B.; Hareau, G.; Julia, S. A.; Lorne, R.; Ruel, O.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 856 - 878
反应条件
samarium diiodide in tetrahydrofuran
Ambient temperature;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa
Tetrahedron Letters, 1995 , vol. 36, # 33 p. 5937 - 5938
