N-(2-羟乙基)六亚甲二胺合成路线 （共 8 条）
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 458;engl.Ausg.S.517
US2735847 , ;
US2743269 , ;
Journal of the American Chemical Society, , vol. 77, p. 1565,1566
反应条件
potassium hydroxide; tetracarbonylhydridoferrate(0); carbon monoxide in ethanol 24 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, p. 1383 - 1385
参考文献
Zhurnal Obshchei Khimii, , vol. 29, p. 631,632; engl. Ausg. S. 626, 627
反应条件
thionyl chloride; benzene
参考文献
Journal of the American Chemical Society, , vol. 80, p. 3729,3730
US2735847 , ;
US2743269 , ;
反应条件
thionyl chloride in chloroform RefluxCooling with ice;
参考文献
Xiao, Chunsheng; Cheng, Yilong; Zhang, Yu; Ding, Jianxun; He, Chaoliang; Zhuang, Xiuli; Chen, Xuesi
Journal of Polymer Science, Part A: Polymer Chemistry, 2014 , vol. 52, # 5 p. 671 - 679
反应条件
1: thionyl chloride / chloroform / |Reflux; |Cooling with ice 2: sodium azide / water / 80 °C View Scheme
参考文献
Xiao, Chunsheng; Cheng, Yilong; Zhang, Yu; Ding, Jianxun; He, Chaoliang; Zhuang, Xiuli; Chen, Xuesi
Journal of Polymer Science, Part A: Polymer Chemistry, 2014 , vol. 52, # 5 p. 671 - 679
反应条件
potassium carbonate
T=160°C;
参考文献
Blicke; Toy
Journal of the American Chemical Society, 1954 , vol. 76, p. 4615
反应条件
sodium methylate in benzene
1.) 0 deg C, 2.) reflux;
参考文献
Kumar, A.; Gurtu, S.; Sinha, J. N.; Bhargava, K. P.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 10 p. 1072 - 1073
