1,3-二(三甲基甲硅烷基)苯合成路线 （共 13 条）
参考文献
Gmelin Handbook: Si: MVol.C, 32, page 100 - 103
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Dow Corning Corp.
Patent: US2628242 , 1953 ;
C. A., 1953 , p. 9346
反应条件
di-tert-butyl peroxide T=130°C; 6.5 h;
参考文献
Sakurai, Hideki; Kira, Mitsuo; Sugiyama, Hisashi
Chemistry Letters, 1983 , p. 599 - 602
反应条件
magnesium in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Yamakawa, Takeru; Kagechika, Hiroyuki; Kawachi, Emiko; Hashimoto, Yuichi; Shudo, Koichi
Journal of Medicinal Chemistry, 1990 , vol. 33, # 5 p. 1430 - 1437
参考文献
Eaborn,C. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1969 , p. 15 - 20
参考文献
Sander,M.
Chemische Berichte, 1962 , vol. 95, p. 473 - 482
反应条件
n-butyllithium; potassium tert-butylate multistep reaction; variation of condition; selective mono- or dimetalation; Product distribution;
参考文献
Schlosser, Manfred; Choi, Jung Hoon; Takagishi, Sadahito
Tetrahedron, 1990 , vol. 46, # 16 p. 5633 - 5648
反应条件
1.1: BCl3 / CH2Cl2 / 10 h / 25 °C 2.1: Br2 / 16 h / 25 °C 3.1: i-Pr2Zn / diethyl ether / 2 h / 25 °C 3.2: CuCN*2LiCl / tetrahydrofuran / 0.17 h / -30 °C 3.3: 56 percent / tetrahydrofuran / 20 °C View Scheme
参考文献
Hupe, Eike; Calaza, M. Isabel; Knochel, Paul
Chemical Communications, 2002 , # 13 p. 1390 - 1391
反应条件
AlCl3, aluminium chloride in dichloromethane T=-12 - -10°C; Friedel-Crafts Acylation; 8.33333 h;
参考文献
Organic Process Research and Development, , vol. 12, # 1 p. 23 - 29
反应条件
AlCl3, aluminium chloride in dichloromethane T=-12 - -10°C; Friedel-Crafts Acylation; 8.33333 h;
参考文献
Wolf, Richard A.
Organic Process Research and Development, 2008 , vol. 12, # 1 p. 23 - 29
参考文献
Felix,G. et al.
Angewandte Chemie, 1977 , vol. 89, p. 502 - 504
