3-(3,4-二甲氧基苯基)丙烯酸乙酯合成路线 (共 28 条)
反应条件
1: potassium hydroxide; methanol 2: sodium amalgam; alkali 3: benzene; P2O5 View Scheme
参考文献
Perkin; Robinson
Journal of the Chemical Society, 1907 , vol. 91, p. 1079
反应条件
sodium hydroxide in ethanol; water T=60°C;
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6713 - 6716
反应条件
methanol; potassium hydroxide
参考文献
Sharma, Mukul; Rajesh, U. Chinna; Rawat, Diwan S.
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1853 - 1860
反应条件
1: 81 percent / LiAlH4 / diethyl ether / 4 h / 0 °C
2: 72 percent / SOCl2, pyridine / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Drewes, Siegfried E.; Hall, Alida J.; Learmonth, Robin A.; Upfold, Ursula J.
Phytochemistry (Elsevier), 1984 , vol. 23, # 6 p. 1313 - 1316
反应条件
hydrogen; palladium on activated charcoal in ethanol; dichloromethane
P=760.051 Torr;
参考文献
Lebel, Helene; Ladjel, Chehla; Brethous, Lise
Journal of the American Chemical Society, 2007 , vol. 129, # 43 p. 13321 - 13326
反应条件
(i) (electrochemical reduction), (ii) /BRN= 1718733/, H2SO4; Multistep reaction;
参考文献
Klemm,L.H.; Olson,D.R.
Journal of Organic Chemistry, 1973 , vol. 38, # 19 p. 3390 - 3394
反应条件
1: LiAlH4 / diethyl ether / -10 °C
2: MnO2 / CCl4 / 0.75 h / Ambient temperature
View Scheme
参考文献
Barcelos, Rosimeire Coura; Pastre, Julio Cezar; Caixeta, Vanessa; Vendramini-Costa, Debora Barbosa; De Carvalho, Joao Ernesto; Pilli, Ronaldo Aloise
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 11 p. 3635 - 3651
反应条件
sodium tetrahydroborate; CoCl2.6H2O; diisopropylamine in ethanol
T=50°C; 24 h; chemoselective reaction;
参考文献
Jagdale, Arun R.; Paraskar, Abhimanyu S.; Sudalai, Arumugam
Synthesis, 2009 , # 4 p. 660 - 664