苯并咪唑并[1,2-a]喹啉合成路线 （共 12 条）
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=120°C; 1 h; Reagent/catalystTemperatureSolventTime;
参考文献
Kato, Jun-Ya; Ito, Yutaro; Ijuin, Ryosuke; Aoyama, Hiroshi; Yokomatsu, Tsutomu
Organic Letters, 2013 , vol. 15, # 14 p. 3794 - 3797
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=120°C;
参考文献
Kato, Jun-Ya; Ito, Yutaro; Ijuin, Ryosuke; Aoyama, Hiroshi; Yokomatsu, Tsutomu
Organic Letters, 2013 , vol. 15, # 14 p. 3794 - 3797
反应条件
peracetic acid; iodobenzene
T=25°C; 1.5 h;
参考文献
He, Yimiao; Huang, Jinbo; Liang, Dongdong; Liu, Lanying; Zhu, Qiang
Chemical Communications, 2013 , vol. 49, # 66 p. 7352 - 7354
反应条件
copper(l) iodide; potassium carbonate; L-proline in acetonitrile
T=76°C; intramolecular Ullmann-type coupling; Inert atmosphere;
参考文献
Zhou, Bing-Wei; Gao, Jian-Rong; Jiang, Dong; Jia, Jian-Hong; Yang, Zhen-Ping; Jin, Hong-Wei
Synthesis, 2010 , # 16 art. no. P04410SS, p. 2794 - 2798
反应条件
PhI(OPiv)2
T=25°C; 10 h;
参考文献
Liang, Dongdong; He, Yimiao; Liu, Lanying; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 13 p. 3476 - 3479
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide
T=130 - 140°C; Buchwald-Harwtig aryl amination; 12 h;
参考文献
Venkatesh; Sundaram; Ila; Junjappa
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1280 - 1283
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide
T=130 - 140°C; Buchwald-Harwtig aryl amination; 12 h;
参考文献
Venkatesh; Sundaram; Ila; Junjappa
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1280 - 1283
反应条件
1: copper; caesium acetate / dimethyl sulfoxide / 24 h / 90 °C / |Inert atmosphere
2: PhI(OPiv)2 / 10 h / 25 °C
View Scheme
参考文献
Liang, Dongdong; He, Yimiao; Liu, Lanying; Zhu, Qiang
Organic Letters, 2013 , vol. 15, # 13 p. 3476 - 3479
反应条件
K-16 in benzene
T=560 - 580°C; 3 h;
参考文献
Varlamov; Krapivko; N'ende; Levov; Prostakov
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 4 p. 459 - 461
反应条件
1: 80 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 20 °C
2: 75 percent / 160 - 170 °C
3: 55 percent / Pd(PPh3)4; K2CO3 / dimethylformamide / 12 h / 130 - 140 °C
View Scheme
参考文献
Venkatesh; Sundaram; Ila; Junjappa
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1280 - 1283
