吲哚(2,3-b)环庚烯合成路线 (共 30 条)
反应条件
L-(+)-tartaric acid-urea melt T=70°C; Fischer Indole Synthesis; 1 h;
参考文献
Gore, Sangram; Baskaran, Sundarababu; Koenig, Burkhard
Organic Letters, 2012 , vol. 14, # 17 p. 4568 - 4571
反应条件
trichloroacetic acid T=100°C; Fischer indole synthesis; 0.0833333 h;
参考文献
Matsumoto, Kiyoshi; Tanaka, Akinori; Yukio, Ikemi; Hayashi, Naoto; Toda, Mitsuo; Bulman, Robert A.
Heterocyclic Communications, 2003 , vol. 9, # 1 p. 9 - 12
反应条件
hydrogen; palladium on activated charcoal in methanol 0.75 h;
参考文献
Banwell, Martin G.; Kelly, Brian D.; Kokas, Okanya J.; Lupton, David W.
Organic Letters, 2003 , vol. 5, # 14 p. 2497 - 2500
反应条件
Cu2Cl2; methyl-magnesium iodide in toluene T=120°C; 2 h;
参考文献
Rodriguez, Gonzalo; Benito, Yolanda; Temprano, Fernando
Chemistry Letters, 1985 , p. 427 - 428
反应条件
hydrogen; toluene-4-sulfonic acid; [rhodium(I)(carbonyl)2(acetylacetonate)] in 1,4-dioxane T=100°C; P=52504.2 Torr; 24 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 2 p. 302 - 313
反应条件
FeBr2 in toluene T=140°C; 16 h; Schlenk techniqueInert atmosphere;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
tris-(2-chloro-ethyl)-amine; sulfuric acid in benzene
参考文献
Adam, G.; Andrieux, J.; Plat, M
Tetrahedron, 1985 , vol. 41, # 2 p. 399 - 408
反应条件
sulfuric acid in 1,4-dioxane 3 h; Heating;
参考文献
Linnepe, Petra; Schmidt, Axel M.; Eilbracht, Peter
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 2 p. 302 - 313
反应条件
1: 66 percent / Cu powder / Pd(dba)2 / dimethylsulfoxide / 1 h / 70 °C 2: 72 percent / H2 / 10 percent Pd/C / methanol / 0.75 h View Scheme
参考文献
Organic Letters, , vol. 5, # 14 p. 2497 - 2500
反应条件
1: 66 percent / Cu powder / Pd(dba)2 / dimethylsulfoxide / 1 h / 70 °C 2: 72 percent / H2 / 10 percent Pd/C / methanol / 0.75 h View Scheme
参考文献
Organic Letters, , vol. 5, # 14 p. 2497 - 2500