1,2-二(苯基)丙-1-酮合成路线 (共 138 条)
反应条件
pyridine
T=0°C; 4.5 h;
参考文献
Sakakura, Toshiyasu; Hara, Masayasu; Tanaka, Masato
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 3 p. 283 - 288
反应条件
potassium dichromate; sulfuric acid
参考文献
Christol,H. et al.
Bulletin de la Societe Chimique de France, 1963 , p. 877 - 881
反应条件
sodium hydroxide; anhydrous tetramethylammonium chloride in toluene
T=60°C; 6 h; various other catalysts; Product distribution;
参考文献
Dehmlow, Eckehard V.; Schrader, Sabine
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 3 p. 409 - 412
反应条件
oxygen; methylene blue in acetonitrile-D3
T=-15°C; 0.333333 h; Irradiation;
参考文献
Sivaguru; Poon, Thomas; Hooper, Catherine; Saito, Hideaki; Solomon, Marissa R.; Jockusch, Steffen; Adam, Waldemar; Inoue, Yoshihisa; Turro, Nicholas J.
Tetrahedron, 2006 , vol. 62, # 46 p. 10647 - 10659
参考文献
Bornstein,J. et al.
Journal of the American Chemical Society, 1963 , vol. 85, p. 1609 - 1615
反应条件
1: AlCl3 / Friedel-Crafts acylation
2: NaOH / neat (no solvent) / 25 deg C, 2h; 100 deg C, 3 h; method of Schultz et al.
View Scheme
参考文献
Dommroese, Anne-Marie; Gruetzmacher, Hans-Friedrich
Organic Mass Spectrometry, 1987 , vol. 22, p. 437 - 443
反应条件
1: AlCl3 / Friedel-Crafts acylation
2: NaOH / neat (no solvent) / 25 deg C, 2h; 100 deg C, 3 h; method of Schultz et al.
View Scheme
参考文献
Dommroese, Anne-Marie; Gruetzmacher, Hans-Friedrich
Organic Mass Spectrometry, 1987 , vol. 22, p. 437 - 443
反应条件
1: diethyl ether
2: H2SO4
View Scheme
参考文献
Ashby,E.C.; Willard,G.F.
Journal of Organic Chemistry, 1978 , vol. 43, # 25 p. 4750 - 4758
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Ashby,E.C. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 1221 - 1232
反应条件
benzene
Behandeln des Reaktionsgemisches mit wss. HCl und anschliessend Erhitzen auf Siedetemperatur;
参考文献
Newman; Linsk
Journal of the American Chemical Society, 1949 , vol. 71, p. 936
反应条件
in diethyl ether; benzene
参考文献
Sawaki,Y.; Ogata,Y.
Journal of the American Chemical Society, 1975 , vol. 97, # 24 p. 6983 - 6989