[(2,6-bis[(di-tert-butylphosphino)methyl]pyridine)Rh(I)(OC6H5)] in tetrahydrofuran; deuterated toluene (N2); using Schlenk techniques; charging of NMR tube with H2O and toluene-d8; degassing, addn. of (C5H3N(CH2P(t-Bu)2)2)Rh(OC6H5) and THF, placing under Ar; heating at 100°C in stainless steel jacket for 360 h; monitoring by NMR;
参考文献
Hanson, Susan Kloek; Heinekey, D. Michael; Goldberg, Karen I.
Organometallics, 2008 , vol. 27, # 7 p. 1454 - 1463
