3，4，5-三甲氧基肉桂酸合成路线 （共 41 条）
反应条件
1: triethylamine / dichloromethane / 2 h / 20 °C / Cooling with ice 2: dichloromethane / 20 °C / Cooling with ice View Scheme
参考文献
Jung, Jae-Chul; Min, Dongguk; Lim, Heena; Moon, Sohyeon; Jung, Mankil; Oh, Seikwan
Medicinal Chemistry Research, 2013 , vol. 22, # 10 p. 4615 - 4621
反应条件
1: 81 percent / H2SO4 / Heating 2: 100 percent / DIBAL-H / CH2Cl2; toluene / 1.5 h / -78 °C 3: MnO2 / ethyl acetate View Scheme
参考文献
Labruere, Raphael; Gautier, Benoit; Testud, Marlene; Seguin, Johanne; Lenoir, Christine; Desbene-Finck, Stephanie; Helissey, Philippe; Garbay, Christiane; Chabot, Guy G.; Vidal, Michel; Giorgi-Renault, Sylviane
ChemMedChem, 2010 , vol. 5, # 12 p. 2016 - 2025
反应条件
1: 3-(3,4,5-trimethoxyphenyl)-2-propenoic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in dichloromethane T=20°C; 0.5 h; 2: pyrrolidine in dichloromethane T=20°C; 24 h;
参考文献
Jung, Jae-Chul; Moon, Sohyeon; Min, Dongguk; Park, Woo Kyu; Jung, Mankil; Oh, Seikwan
Chemical Biology and Drug Design, 2013 , vol. 81, # 3 p. 389 - 398
反应条件
1: triethylamine / tetrahydrofuran / 0.75 h / -20 °C 2: triethylamine / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Rao, Vidadala Ramasubba; Muthenna, Puppala; Shankaraiah, Gundeti; Akileshwari, Chandrasekhar; Babu, Kothapalli Hari; Suresh, Ganji; Babu, Katragadda Suresh; Chandra Kumar, Rotte Sateesh; Prasad, Kothakonda Rajendra; Yadav, Potharaju Ashok; Petrash, J. Mark; Reddy, Geereddy Bhanuprakash; Rao, Janaswamy Madhusudana
European Journal of Medicinal Chemistry, 2012 , vol. 57, p. 344 - 361
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Hu, Li Hong; Zou, Hong Bin; Gong, Jing Xu; Li, Hai Bo; Yang, Lei Xiang; Cheng, Wei; Zhou, Chang Xin; Bai, Hua; Gueritte, Francoise; Zhao, Yu
Journal of Natural Products, 2005 , vol. 68, # 3 p. 342 - 348
反应条件
hydrogenchloride; sodium borohydride; triethylamine in tetrahydrofuran
参考文献
Kowa Co., Ltd.
Patent: US2003/22887 A1, 2003 ;
反应条件
formic acid; palladium dichloride in sodium hydroxide; isopropyl alcohol 0.05 h; microwave irradiation;
参考文献
Sharma, Anuj; Joshi, Bhupendra P.; Sinha, Arun K.
Chemistry Letters, 2003 , vol. 32, # 12 p. 1186 - 1187
反应条件
sulfuric acid 12 h; Heating;
参考文献
Peterson, John R.; Russell, Morley E.; Surjasasmita, Irawan B.
Journal of Chemical & Engineering Data, 1988 , vol. 33, # 4 p. 534 - 537
参考文献
Banwell, Martin G.; Lambert, John N.; Gravatt, G. Lance
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 22 p. 2817 - 2830
反应条件
sulfuric acid in methanol 5 h; Heating;
参考文献
Rao, Vidadala Ramasubba; Muthenna, Puppala; Shankaraiah, Gundeti; Akileshwari, Chandrasekhar; Babu, Kothapalli Hari; Suresh, Ganji; Babu, Katragadda Suresh; Chandra Kumar, Rotte Sateesh; Prasad, Kothakonda Rajendra; Yadav, Potharaju Ashok; Petrash, J. Mark; Reddy, Geereddy Bhanuprakash; Rao, Janaswamy Madhusudana
European Journal of Medicinal Chemistry, 2012 , vol. 57, p. 344 - 361
