L-(-)-3-苯基乳酸合成路线 (共 71 条)
反应条件
1: 89 percent / acetonitrile / 1.5 h / -45 °C 2: 94 percent / 5 percent KOH / methanol / 3 h / 20 °C View Scheme
参考文献
Chemische Berichte, , vol. 119, # 5 p. 1594 - 1612
反应条件
cellulose-modified silica gel in hexane; isopropyl alcohol Resolution of racemate;
参考文献
Asian Journal of Chemistry, , vol. 24, # 11 p. 4917 - 4922
反应条件
iodoacetate spiropyran modified-Bacillus thermocathenolatus lipase 2 at positon 245 immobilized on transparent agarose microspheres UV-irradiation; Reagent/catalyst; enantioselective reaction;
参考文献
ACS Catalysis, , vol. 4, # 3 p. 1004 - 1009
反应条件
water; sodium carbonate 4 h; Reflux;
参考文献
Rochon, Kristina; Proteau-Gagne, Arnaud; Bourassa, Philippe; Nadon, Jean-Francois; Coite, Jerome; Bournival, Veronique; Gobeil, Fernand; Guerin, Brigitte; Dory, Yves L.; Gendron, Louis
ACS Chemical Neuroscience, 2013 , vol. 4, # 8 p. 1204 - 1216
反应条件
sulfuric acid 24 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 25, # 1 p. 39 - 42
反应条件
1: grassypeptolide D With ozone in dichloromethane T=-78°C; 0.25 h; 2: With formic acid; dihydrogen peroxide in water T=70°C; 0.333333 h; 3: Nα-(2,4-dinito-5-fluorophenyl)-L-leucinamide Further stages;
参考文献
Journal of Natural Products, , vol. 74, # 8 p. 1677 - 1685
反应条件
1: grassypeptolide E With ozone in dichloromethane T=-78°C; 0.25 h; 2: With formic acid; dihydrogen peroxide in water T=70°C; 0.333333 h; 3: Nα-(2,4-dinito-5-fluorophenyl)-L-leucinamide Further stages;
参考文献
Journal of Natural Products, , vol. 74, # 8 p. 1677 - 1685
参考文献
Acta Sch. med. Univ. Kioto, vol. 2, p. 449,455
Chem. Zentralbl., , vol. 91, # III p. 489
反应条件
Pseudomonas sp. BC-18 T=30°C; 4 h; phosphate buffer, borate buffer; pH 9.0;
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 60, # 8 p. 1279 - 1283
反应条件
1: L-phenylalanine Diazotization; 2: Hydrolysis; 3: ethanol Esterification;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 19 p. 3747 - 3758