N-氰甲基-4-甲基苯磺酰胺合成路线 (共 6 条)
反应条件
in pyridine T=0°C; 0.5 h;
参考文献
SMITHKLINE BEECHAM CORPORATION
Patent: WO2004/101512 A2, 2004 ;
Location in patent: Page 53 ;
反应条件
pyridine T=0°C; 0.5 h;
参考文献
Johns, Brian A.; Weatherhead, Jason G.; Allen, Scott H.; Thompson, James B.; Garvey, Edward P.; Foster, Scott A.; Jeffrey, Jerry L.; Miller, Wayne H.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 6 p. 1802 - 1806
反应条件
in dimethyl sulfoxide 24 h;
参考文献
Katritzky, Alan R.; Oniciu, Daniela C.; Ghiviriga, Ion
Synthetic Communications, 1997 , vol. 27, # 5 p. 907 - 922
反应条件
1: 95 percent / ethanol; H2O / 48 h / Ambient temperature 2: 80 percent / dimethylsulfoxide / 24 h View Scheme
参考文献
Katritzky, Alan R.; Oniciu, Daniela C.; Ghiviriga, Ion
Synthetic Communications, 1997 , vol. 27, # 5 p. 907 - 922
反应条件
sodium hydrogencarbonate
参考文献
Suzue; Irikura
Chemical and pharmaceutical bulletin, 1968 , vol. 16, # 8 p. 1417 - 1432
参考文献
Farbw.Hoechst
Patent: DE847006 , 1951 ;
DRP/DRBP Org.Chem.