1-氨基-2,4-二溴萘合成路线 （共 14 条）
参考文献
Franzen; Staeuble
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 103, p. 367
反应条件
sulfuric acid Diazotization;
参考文献
Meldola
Journal of the Chemical Society, 1884 , vol. 45, p. 161
反应条件
N-bromosuccinmide; lithium perchlorate; silica gel in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Bagheri, Mojtaba; Azizi, Najmedin; Saidi, Mohammad R.
Canadian Journal of Chemistry, 2005 , vol. 83, # 2 p. 146 - 149
反应条件
1: With n-butyllithium in diethyl ether; hexane
T=-78°C; 1 h;
2: With poly[4-(dibutyliodostannyl)butyl]styrene in diethyl ether; hexane
T=20°C; 18 h;
3: With bromine in diethyl ether; hexane; dichloromethane
T=-78 - 20°C; 2 h;
参考文献
Chretien, Jean-Mathieu; Zammattio, Francoise; Le Grognec, Erwan; Paris, Michael; Cahingt, Blanche; Montavon, Gilles; Quintard, Jean-Paul
Journal of Organic Chemistry, 2005 , vol. 70, # 7 p. 2870 - 2873
反应条件
chloroform; bromine
T=0°C;
参考文献
Rowe; Davies
Journal of the Chemical Society, 1922 , vol. 121, p. 1006
反应条件
sodium hydroxide
T=140 - 150°C;
参考文献
Meldola
Chemische Berichte, 1878 , vol. 11, p. 1961
反应条件
bromine; acetic acid
参考文献
Heller
Angewandte Chemie, 1930 , vol. 43, p. 1132,1133
反应条件
chloroform; bromine
durch Zusatz von Pyridin erneute Behandlung mit Brom und Kochen der Reaktionsfluessigkeit nach Zusatz von absol.Alkohol;
参考文献
Franzen; Aaslund
Journal fuer Praktische Chemie (Leipzig), 1917 , vol. <2> 95, p. 163
参考文献
Rowe; Davies
Journal of the Chemical Society, 1922 , vol. 121, p. 1006
参考文献
Ruggli; Braun
Helvetica Chimica Acta, 1933 , vol. 16, p. 858,863
