1-甲基肼-1-二硫代羧酸甲酯合成路线 （共 16 条）
反应条件
acetic acid in ethanol 4 h; Heating;
参考文献
Scovill, John P.; Silverton, J.V.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4372 - 4376
反应条件
1: carbon disulfide; methylhydrazine With potassium hydroxide in ethanol
1 h;
2: methyl iodide in water
T=10 - 15°C; 3 h;
参考文献
WARNER-LAMBERT COMPANY
Patent: EP1193261 A1, 2002 ;
Location in patent: Page 18 ;
EP 1193261 A1
反应条件
in N,N-dimethyl-formamide
T=0°C; 0.5 h; Yields of byproduct given;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
1 h; Ambient temperature; Yields of byproduct given;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
8 h; Ambient temperature; Yields of byproduct given;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
4 h; Ambient temperature;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
4 h; Ambient temperature;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
5 h; Ambient temperature; Yields of byproduct given;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
20 h; Ambient temperature;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
反应条件
in methanol
6 h; Ambient temperature; Yields of byproduct given;
参考文献
Barkoczy, Jozsef; Reiter, Jozsef
Journal of Heterocyclic Chemistry, 1992 , vol. 29, p. 1677 - 1683
