2,2-二氯丙二酸二乙酯合成路线 （共 23 条）
反应条件
tris-(dimethylamino)-phosphine in tetrahydrofuran T=-35 - 24°C;
参考文献
Vorbruggen; Bohn; Krolikiewicz
Tetrahedron, 1990 , vol. 46, # 10 p. 3489 - 3502
反应条件
pentacarbonyliron(0) in N,N-dimethyl-formamide T=150°C; 0.5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 12 p. 2347 - 2349
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2815 - 2818
反应条件
pentacarbonyliron(0) in N,N-dimethyl-formamide T=150°C; 0.5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 12 p. 2347 - 2349
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 12 p. 2815 - 2818
反应条件
pentacarbonyliron(0) in tert-butyl alcohol T=150°C;
参考文献
Velichko,F.K. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1342
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1455
参考文献
Conrad; Brueckner
Chemische Berichte, 1891 , vol. 24, p. 3002
参考文献
Conrad; Brueckner
Chemische Berichte, 1891 , vol. 24, p. 3002
参考文献
Conrad; Brueckner
Chemische Berichte, 1891 , vol. 24, p. 3002
反应条件
1: 1) tris(dimethylamino)phosphine / 1) THF, 1 h, -35 deg C, 2a) THF, 2 h, -30 deg C, 2b) 18 h, 24 deg C 2: 83 percent / tris(dimethylamino)phosphine / tetrahydrofuran / 2 h / -35 °C View Scheme
参考文献
Tetrahedron, , vol. 46, # 10 p. 3489 - 3502
反应条件
manganese; [CpRuCl2(PPh3)] in tetrahydrofuran T=60°C; 2 h; Inert atmosphere;
参考文献
Fernandez-Zumel, Mariano A.; Buron, Charlotte; Severin, Kay
European Journal of Organic Chemistry, 2011 , # 12 p. 2272 - 2277
反应条件
(i) iPrMgCl, THF, (ii) aq. HCl; Multistep reaction;
参考文献
Nicholson,D.A.; Vaughn,H.
Journal of Organic Chemistry, 1971 , vol. 36, # 13 p. 1835 - 1837
