反应条件
1: C21H22OSi With n-butyllithium in tetrahydrofuran; hexane
T=0°C; 0.5 h; Inert atmosphere;
2: 3-chloroprop-1-ene With copper(l) iodide; triethyl phosphite in N,N-dimethyl-formamide
T=50°C; 16 h; Inert atmosphere; Reagent/catalyst;
参考文献
Tsubouchi, Akira; Muramatsu, Daisuke; Takeda, Takeshi
Angewandte Chemie - International Edition, 2013 , vol. 52, # 48 p. 12719 - 12722
Angew. Chem., 2013 , vol. 125, # 48 p. 12951 - 12954,4