2-(苯基甲基)-1,3-苯并恶唑合成路线 (共 32 条)
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in tetrahydrofuran; diethyl ether T=-15°C;
参考文献
Tetrahedron, , vol. 40, # 24 p. 5089 - 5096
反应条件
cerium(IV) oxide in water
T=30°C; 0.5 h;
参考文献
Shelkar, Radheshyam; Sarode, Sachin; Nagarkar, Jayashree
Tetrahedron Letters, 2013 , vol. 54, # 51 p. 6986 - 6990
反应条件
Lawesson's reagent
T=190°C; 0.0333333 h; microwave irradiation;
参考文献
Seijas, Julio A.; Vazquez-Tato, M. Pilar; Carballido-Reboredo, M. Raquel; Crecente-Campo, Jose; Romar-Lopez, Lucia
Synlett, 2007 , # 2 p. 313 - 317
反应条件
dichloro bis(acetonitrile) palladium(II); 1,3-bis-(diphenylphosphino)propane; sodium carbonate in N,N-dimethyl-formamide
T=120°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Xie, Pan; Huang, Hanmin; Xie, Yinjun; Guo, Shengmei; Xia, Chungu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1692 - 1700
反应条件
methanesulfonic acid in 1,4-dioxane
T=100°C; 2 h; chemoselective reaction;
参考文献
Kumar, Dinesh; Rudrawar, Santosh; Chakraborti, Asit K.
Australian Journal of Chemistry, 2008 , vol. 61, # 11 p. 881 - 887
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 1,3-bis-(diphenylphosphino)propane; sodium acetate in dimethyl sulfoxide
T=120°C; 3 h; Inert atmosphere;
参考文献
Mukai, Tomoya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2010 , vol. 12, # 6 p. 1360 - 1363
反应条件
potassium phosphate; palladium diacetate; 1,2-bis-(diphenylphosphino)ethane in 1-methyl-pyrrolidin-2-one
T=100°C; 15 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Barfuesser, Sebastian; Pospech, Jola
Organic Letters, 2010 , vol. 12, # 4 p. 724 - 726
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; 10 palladium on activated carbon in acetic acid
T=120°C; 15 h; Inert atmosphere;
参考文献
Xing, Rui-Guang; Li, Ya-Nan; Liu, Qiang; Meng, Qing-Yuan; Li, Jing; Shen, Xiao-Xia; Liu, Zhengang; Zhou, Bo; Yao, Xiaojun; Liu, Zhong-Li
European Journal of Organic Chemistry, 2010 , # 34 p. 6627 - 6632
反应条件
copper(l) iodide; 1,10-phenanthroline; caesium carbonate in ethylene glycol dimethyl ether
24 h; Heating;
参考文献
Evindar, Ghotas; Batey, Robert A.
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 1802 - 1808
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,3,5-trimethyl-benzene
T=140°C; 10 h; Inert atmosphere;
参考文献
Shang, Rui; Yang, Zhi-Wei; Wang, Yan; Zhang, Song-Lin; Liu, Lei
Journal of the American Chemical Society, 2010 , vol. 132, # 41 p. 14391 - 14393