反应条件
1.1: 45 percent / Et3N / ethanol / 16 h / Heating 2.1: LHMDS / tetrahydrofuran / 1 h / -78 °C 2.2: 94 percent / tetrahydrofuran / 16 h / -78 - 20 °C 3.1: 65 percent / t-BuOK / tetrahydrofuran / 8.5 h / -78 °C 4.1: LDA / hexane; tetrahydrofuran / -78 - 0 °C 4.2: hexane; tetrahydrofuran / 8.5 h / -78 - -30 °C 4.3: 75 mg / ammonium formate / Pd(OH)2/C / ethanol / 4 h / Heating 5.1: 88 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Hermet, Jean-Paul R.; McGrath, Matthew J.; O'Brien, Peter; Porter, David W.; Gilday, John
Chemical Communications, 2004 , # 16 p. 1830 - 1831
