顺式-7-十二碳烯-1-醇合成路线 （共 41 条）
反应条件
1: KOH / methanol / (electrolysis)
2: LiAlH4
View Scheme
参考文献
Seidel,W. et al.
Chemische Berichte, 1977 , vol. 110, p. 3544 - 3552
反应条件
1: potassium meta-periodate; sulfuric acid / water; methanol / 0.17 h / 20 - 40 °C
2: potassium carbonate / toluene / 4 h / |Reflux
View Scheme
参考文献
Majee
Journal of the Indian Chemical Society, 2012 , vol. 89, # 10 p. 1435 - 1438
反应条件
4-bromooctafluorobutanetriethoxysilane; water; hydrogen; Rhodium trichloride; copper(II) nitrate in tetrahydrofuran
Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tour, James M.; Pendalwar, Shekhar L.; Kafka, Cynthia M.; Cooper, Joel P.
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4786 - 4787
反应条件
sodium hydroxide; dihydrogen peroxide; iodine; magnesium; benzo[1,3,2]dioxaborole
2.) THF, 0 deg C then reflux; 3.) THF, 0 deg C; Yield given. Multistep reaction;
参考文献
Periasamy, Mariappan; Bhanu Prasad; Suseela, Yantrapragada
Tetrahedron, 1995 , vol. 51, # 9 p. 2743 - 2748
反应条件
lithium aluminium tetrahydride
参考文献
Seidel,W. et al.
Chemische Berichte, 1977 , vol. 110, p. 3544 - 3552
反应条件
sodium methylsulfinylmethanide in tetrahydrofuran; dimethyl sulfoxide
T=5°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiike; Hirano
Agricultural and Biological Chemistry, 1980 , vol. 44, # 9 p. 2229 - 2230
反应条件
Yield given. Multistep reaction;
参考文献
Basavaiah, D.; Brown, Herbert C.
Journal of Organic Chemistry, 1982 , vol. 47, # 9 p. 1792 - 1793
Title/Abstract Full Text View citing articles Show Details
Brown, Herbert C.; Basavaiah, Deevi; Singh, Shankar M.; Bhat, Narayan G.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 246 - 250
反应条件
1: 73 percent / 4 h / 90 °C
View Scheme
参考文献
Poleschner; Heydenreich; Martin
Synthesis, 1991 , # 12 p. 1231 - 1235
参考文献
Tolstikov, G. A.; Odinokov, V. N.; Galeeva, R. I.; Bakeeva, R. S.; Akhunova, V. R.
Chemistry of Natural Compounds, 1982 , vol. 18, # 2 p. 219 - 224
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 2 p. 239 - 245
反应条件
pyridine in hexane
Acetylation; 2 h;
参考文献
Bykov; Butenko; Egupova; Finkelshtein
Russian Chemical Bulletin, 2000 , vol. 49, # 7 p. 1301 - 1304
