1-(三甲基硅氧基)环戊烯合成路线 （共 155 条）
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prieto, J. Antonio; Larson, Gerald L.
Synthetic Communications, 1980 , vol. 10, # 9 p. 675 - 684
反应条件
in tetrahydrofuran 1) ca. -40 deg C, 1 h 2) r.t., 1 h;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
反应条件
water; hydrogen cation; titanium tetrachloride 1.)CH2Cl2, -70 deg C; Yield given. Multistep reaction;
参考文献
El-Abed, Douniazad; Jellal, Abdelkebir; Santelli, Maurice
Tetrahedron Letters, 1984 , vol. 25, # 40 p. 4503 - 4504
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; methyllithium; dimethyl zinc in tetrahydrofuran T=-78°C; 10 h;
参考文献
Morita, Yasushi; Suzuki, Masaaki; Noyori, Ryoji
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1785 - 1787
反应条件
silver trifluoroacetate in dichloromethane T=25°C; 0.166667 h;
参考文献
Jefford, Charles W.; Sledeski, Adam W.; Lelandais, Patrick; Boukouvalas, John
Tetrahedron Letters, 1992 , vol. 33, # 14 p. 1855 - 1858
反应条件
methyllithium in tetrahydrofuran T=0°C; 3 h; Further byproducts given;
参考文献
Morita, Yasushi; Suzuki, Masaaki; Noyori, Ryoji
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1785 - 1787
反应条件
methyllithium in tetrahydrofuran T=0°C; 3 h; var. temp., times, and reagent systems; other lithium enolates; Product distribution;
参考文献
Morita, Yasushi; Suzuki, Masaaki; Noyori, Ryoji
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1785 - 1787
反应条件
1: triethylamine / hexane 2: acetic acid; zinc / water; isopropyl alcohol View Scheme
参考文献
Ragan, John A.; Murry, Jerry A.; Castaldi, Michael J.; Conrad, Alyson K.; Jones, Brian P.; Bryan, Li; Makowski, Teresa W.; McDermott, Ruth; Sitter, Barb J.; White, Timothy D.; Young, Gregory R.
Organic Process Research and Development, 2001 , vol. 5, # 5 p. 498 - 507
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prieto, J. Antonio; Larson, Gerald L.
Synthetic Communications, 1980 , vol. 10, # 9 p. 675 - 684
反应条件
hydrogenchloride in tetrahydrofuran 0.5 h; Ambient temperature; Yield given;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
