反应条件
1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / ethylene glycol dimethyl ether; water / 5 h / 80 °C / Inert atmosphere 2: hydrogenchloride / methanol; water / 1 h / 20 °C 3: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere 4: tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 15 h / 110 °C / Inert atmosphere 5: potassium tert-butylate / tetrahydrofuran / 8 h / 50 °C / Inert atmosphere View Scheme
参考文献
Jepsen, Tue Heesgaard; Larsen, Mogens; Jorgensen, Morten; Solanko, Katarzyna A.; Bond, Andrew D.; Kadziola, Anders; Nielsen, Mogens Brondsted
European Journal of Organic Chemistry, 2011 , # 1 p. 53 - 57