2,6-二甲氧基苯甲酰氯合成路线 (共 20 条)
反应条件
thionyl chloride Heating;
参考文献
Chemische Berichte, , vol. 99, p. 1906 - 1911
反应条件
thionyl chloride in toluene
参考文献
Journal of the American Chemical Society, , vol. 61, p. 1418
反应条件
pyridine in dichloromethane T=0°C; 1 h;
参考文献
Arrieta, A.; Garcia, T.; Palomo, C.
Synthetic Communications, 1982 , vol. 12, # 14 p. 1139 - 1146
反应条件
water in acetone T=-20°C; Rate constant;
参考文献
Chemische Berichte, , vol. 94, p. 1839 - 1850
反应条件
triethylamine in acetonitrile T=20°C; 3 h;
参考文献
Rivero-Cruz, Blanca; Rivero-Cruz, Isabel; Rodriguez, Juan M.; Cerda-Garcia-Rojas, Carlos M.; Mata, Rachel
Journal of Natural Products, 2006 , vol. 69, # 8 p. 1172 - 1176
反应条件
aluminium trichloride in diethyl ether 12 h; Ambient temperature; Yield given;
参考文献
Tosa, Hideki; Iinuma, Munekazu; Murakami, Koh-Ichi; Ito, Tetsuro; Tanaka, Toshiyuki; Chelladurai, Veliah; Riswan, Soedarsono
Phytochemistry, 1997 , vol. 45, # 1 p. 133 - 136
反应条件
1: 90 percent / 3 h / Ambient temperature 2: 62 percent / HN3, H2SO4 / CHCl3 / 0.08 h / 0 °C View Scheme
参考文献
Sprecher, Milon; Kost, Daniel
Journal of the American Chemical Society, 1994 , vol. 116, # 3 p. 1016 - 1026
反应条件
2,2'-azo-bisisobutyronitrile; trichloromonobromomethane; Fonderma T=100°C; 0.0833333 h; Heating; Yield given. Yields of byproduct given;
参考文献
Barton, Derek H.R.; Lacher, Brigitte; Zard, Samir Z.
Tetrahedron, 1987 , vol. 43, # 19 p. 4321 - 4328
反应条件
indium T=80°C; 3 h; Inert atmosphere;
参考文献
Lo Fiego, Marcos J.; Silbestri, Gustavo F.; Chopa, Alicia B.; Lockhart, Maria T.
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1707 - 1714