N-乙氧羰基-L-苯丙氨酸合成路线 （共 6 条）
反应条件
sodium hydroxide; sodium carbonate in water T=0 - 20°C; 1 h;
参考文献
Xu, Qianyong; Yang, Hongfang; Pan, Xinfu; Chan, Albert S.C.
Tetrahedron Asymmetry, 2002 , vol. 13, # 9 p. 945 - 951
反应条件
triethylamine in methanol T=20°C; 3 h;
参考文献
Kita, Yasuyuki; Haruta, Jun-ichi; Tagawa, Hiroko; Tamura, Yasumitsu
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4519 - 4522
反应条件
hydrogenchloride; potassium chloride; tri-(hydroxymethyl)-methylamine; S12-L-Phe-L-His-L-Leu in water; acetonitrile T=25°C; pH 7.3, surfactant R-surf 16; k(L)/k(D), ΔΔG(excit.); Rate constant;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 111, # 11 p. 459 - 468
反应条件
PTC; S4-L-Phe-L-His-L-Leu in water; acetonitrile T=25°C; pH 7.3; Rate constant;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 1 p. 1 - 6
反应条件
in tetrahydrofuran; water T=0°C; 0.5 h;
参考文献
Chemistry Letters, , vol. 41, # 1 p. 42 - 43
→
857637-92-44-苄基-5-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)-1,3-恶唑烷-2-酮
反应条件
1: iBuCOCl
2: LiAlH(OtBu)3
3: NaH / tetrahydrofuran
View Scheme
参考文献
Hein, Jason E.; Geary, Laina M.; Jaworski, Ashley A.; Hultin, Philip G.
Journal of Organic Chemistry, 2005 , vol. 70, # 24 p. 9940 - 9946
