1-乙基六氢-2H-氮杂卓-2-酮合成路线 （共 8 条）
反应条件
silver tetrafluoroborate; Br(1-)*C29H31BrN5Pt(1+) in PhNO2-d5 T=20 - 150°C; P=4125.41 Torr; 26 h; Inert atmosphere;
参考文献
Cao, Peng; Cabrera, Jose; Padilla, Robin; Serra, Daniel; Rominger, Frank; Limbach, Michael
Organometallics, 2012 , vol. 31, # 3 p. 921 - 929
反应条件
ammonium formate; palladium on activated charcoal in methanol 0.5 h; Heating;
参考文献
Paryzek, Zdzislaw; Koenig, Hanna; Tabaczka, Bartlomiej
Synthesis, 2003 , # 13 p. 2023 - 2026
反应条件
T=180 - 250°C; unter Stickstoff;
参考文献
Benson; Cairns
Journal of the American Chemical Society, 1948 , vol. 70, p. 2115,2116
Org.Synth.Coll.Vol., 1963 , vol. IV, p. 588
反应条件
1: benzene 2: 180 - 250 °C / unter Stickstoff View Scheme
参考文献
Benson; Cairns
Journal of the American Chemical Society, 1948 , vol. 70, p. 2115,2116
Org.Synth.Coll.Vol., 1963 , vol. IV, p. 588
反应条件
aluminum oxide T=350°C;
参考文献
Schpital'nyi; Kusnezowa
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1957 , vol. 30, p. 1848; engl. Ausg. S. 1916
反应条件
sodium hydride 1) toluene, reflux, 1 h; 2) toluene, 2 h (room temperature), reflux (8 h); Yield given. Multistep reaction;
参考文献
Ponec; Haverkort; Soei; Kempenaar; Brussee; Bodde
Journal of Pharmaceutical Sciences, 1989 , vol. 78, # 9 p. 738 - 741
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate 73 h; Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 35, # 1 p. 357 - 363
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate
73 h; Ambient temperature;
参考文献
Yoshifuji, Shigeyuki; Arakawa, Yukimi; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 1 p. 357 - 363
