pyridine; 3 A molecular sieve; oxygen; palladium (II) trifluoroacetate; sodium carbonate in toluene
T=80°C; P=760 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Trend, Raissa M.; Ramtohul, Yeeman K.; Stoltz, Brian M.
Journal of the American Chemical Society, 2005 , vol. 127, # 50 p. 17778 - 17788
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane
0.583333 h;
2: With sodium potassium tartrate in tetrahydrofuran; hexane; water
T=20°C; 0.25 h;
参考文献
Faulkner, Adele; Bower, John F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 7 p. 1675 - 1679