3-(1-哌啶基)-丙酸乙酯合成路线 (共 26 条)
反应条件
anhydrous cobalt diacetate in water T=20°C; aza-type Michael addition; 15 h;
参考文献
Duan, Zheng; Xuan, Xuejie; Li, Ting; Yang, Chenfei; Wu, Yangjie
Tetrahedron Letters, 2006 , vol. 47, # 31 p. 5433 - 5436
反应条件
hafnium triflate in dichloromethane T=20°C; Mannich type reaction; 1 h;
参考文献
Sakai, Norio; Sato, Asuka; Konakahara, Takeo
Synlett, 2009 , # 9 p. 1449 - 1452
反应条件
sodium cyanoborohydride 1.) ethanol; 2.) ethanolic HCl, overnight;
参考文献
Sundberg, Richard J.; Walters, Claudia Powers; Bloom, Jonathan D.
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3730 - 3732
反应条件
1: absolute ether; HBr / erst unter Eiskuehlung, zuletzt bei Raumtemperatur View Scheme
参考文献
Journal of the American Chemical Society, , vol. 56, p. 698
参考文献
Journal of the American Chemical Society, , vol. 51, p. 602
参考文献
Journal of the American Chemical Society, , vol. 67, p. 1071,1972
反应条件
1: tetrahydrofuran 2: 53 percent / NaBH3CN / 1.) ethanol; 2.) ethanolic HCl, overnight View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 18 p. 3730 - 3732
反应条件
1: 76 percent / P2S5 / toluene / 1 h / Ambient temperature 2: tetrahydrofuran 3: 53 percent / NaBH3CN / 1.) ethanol; 2.) ethanolic HCl, overnight View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 18 p. 3730 - 3732
参考文献
Chemische Berichte, , vol. 59, p. 1946
Journal of the American Chemical Society, , vol. 51, p. 601
Chemische Berichte, , vol. 62, p. 1694
参考文献
Journal of the American Chemical Society, , vol. 56, p. 698