2-甲基-5-溴苯并咪唑合成路线 (共 13 条)
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane T=20 - 100°C; 1 h; Inert atmosphere;
参考文献
Bommegowda, Yadaganahalli K.; Lingaraju, Gejjalagere S.; Thamas, Saji; Vinay Kumar, Koravangala S.; Pradeepa Kumara, Challanayakanahally S.; Rangappa, Kanchugarakoppal S.; Sadashiva, Marilinganadoddi P.
Tetrahedron Letters, 2013 , vol. 54, # 21 p. 2693 - 2695
反应条件
indium; acetic acid in ethyl acetate 4 h; RefluxInert atmosphere;
参考文献
Kim, Jaeho; Kim, Jihye; Lee, Hyunseung; Lee, Byung Min; Kim, Byeong Hyo
Tetrahedron, 2011 , vol. 67, # 41 p. 8027 - 8033
反应条件
RefluxInert atmosphereSchlenk technique;
参考文献
Huynh, Han Vinh; Ong, Hong Lee; Bernhammer, Jan C.; Frison, Gilles
European Journal of Inorganic Chemistry, 2013 , # 26 p. 4654 - 4661
反应条件
N-bromosuccinmide; silica gel in dichloromethane T=20°C; 1 h;
参考文献
Mistry, Anil G.; Smith, Keith; Bye, Martin R.
Tetrahedron Letters, 1986 , vol. 27, # 9 p. 1051 - 1054
反应条件
caesium carbonate; copper(I) bromide in dimethyl sulfoxide T=70 - 120°C; 72 h;
参考文献
Yang, Daoshan; Fu, Hua; Hu, Liming; Jiang, Yuyang; Zhao, Yufen
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7841 - 7844
反应条件
in water T=100°C; 15 h;
参考文献
WO2008/124849 A2, ;
Page/Page column 89 ;
WO 2008/124849 A2
反应条件
hydrogenchloride; tin
参考文献
Chemische Berichte, , vol. 7, p. 348
参考文献
Journal of the Chemical Society, , p. 1143,1153
参考文献
Chemische Berichte, , vol. 38, p. 327
参考文献
Chim. farm. Z., , vol. 9, # 9 p. 18; engl. Ausg. S. 565