3,5-二甲基-4-亚硝基苯酚合成路线 (共 9 条)
反应条件
hydrogenchloride; sodium nitrite in ethanol; water T=0°C; Inert atmosphere;
参考文献
Schmidt, Bernd; Berger, Rene; Kelling, Alexandra; Schilde, Uwe
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 7032 - 7040
反应条件
sodium ethanolate in dimethyl sulfoxide 1 h;
参考文献
Belyaev, E. Yu.; El'tsov, A. V.; Kochetkov, B. B.; Orlovskaya, N. F.; Tovbis, M. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1299 - 1304
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1489 - 1495
反应条件
potassium tert-butylate in tert-butyl alcohol var. reagents, var. solvents; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 18, p. 1299 - 1304
Zhurnal Organicheskoi Khimii, , vol. 18, # 7 p. 1489 - 1495
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1330
反应条件
palladium on carbon; hydrogen in ethyl acetate P=750.075 Torr; 2 h;
参考文献
Schmidt, Bernd; Berger, Rene; Kelling, Alexandra; Schilde, Uwe
Chemistry - A European Journal, 2011 , vol. 17, # 25 p. 7032 - 7040
反应条件
1: sodium dithionite; aq. NaOH solution View Scheme
参考文献
Rowe et al.
Journal of the Society of Chemical Industry, London, 1930 , vol. 49, p. 469 T, 472 T
反应条件
1: aqueous NH3; H2S
2: aqueous HCl; sodium acetate
View Scheme
参考文献
Loefgren; Tegner
Acta Chemica Scandinavica (1947-1973), 1954 , vol. 8, p. 1802,1805
反应条件
dihydrogen peroxide; acetic acid; (NH4)6[Mo7O24]*4H2O
T=100°C;
参考文献
VALEANT PHARMACEUTICALS INTERNATIONAL
Patent: US2009/326059 A1, 2009 ;
Location in patent: Page/Page column 16 ;
US 20090326059 A1
反应条件
in acetic acid; toluene
参考文献
William H. Rorer, Inc.
Patent: US4487779 A1, 1984 ;